Organic Communications

Year: 2014  Volume: 7  Issue: 1

 

  ORIGINAL ARTICLE

2.

Stereoselective synthesis of tuberculostatic agent (S,S)-ethambutol

J. Kranthi Kumar and A. Venkat Narsaiah

Organic and Biomolecular Chemistry Division, Indian Institute of Chemical Technology, Hyderabad-500007, INDIA

Abstract: A simple and efficient asymmetric synthesis of (S,S)-Ethambutol has been carried out using a chiral butanediol. The synthesis was completed within six steps with an overall yield 53% and the enantiomeric purity of final product was 98%. All the reactions were very clean and the yields are excellent.

Keywords: Ethambutol; butanediol; protection; tuberculosis; oxalylchloride; reduction. © 2014 ACG Publications. All rights reserved.