Microwave-assisted preparation of graphene quantum dots immobilized nanosilica as an efficient heterogeneous nanocatalyst for the synthesis of xanthenes
Available Online: March 01,2019
p.1 - 12
http://doi.org/10.25135/acg.oc.126.96.36.1991 (DOI number will be activated after the manuscript has been available in an issue.)
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- 1 - Azarbaijan Shahid Madani University
- 2 - Azarbaijan Shahid Madani University
Abstract: Graphene quantum dots (GQDs) immobilized nanosilica was prepared under microwave irradiated green reaction conditions and was used as an efficient heterogeneous acid catalyst. The structure of nano-catalyst was characterized by FT-IR, PL, TEM, XRD, FE-SEM, EDS, TGA, and zeta potential. Xanthene derivatives were synthesized in excellent yields using the freshly prepared catalyst and the catalyst could be easily recovered and recycled for 5 times without significant loss of its catalytic activity. The structures of the resulted products were confirmed by FT-IR, 1H-NMR, 13C-NMR spectroscopic techniques.
- Graphene quantum dots
- heterogeneous nanocatalyst