JOURNAL 3177


Organic Communications
VOLUME & ISSUE
Available Online: May 13,2024
PAGES
p.1 - 5
DOI ADDRESS
http://doi.org/10.25135/acg.oc.166.2403.3177
(DOI number will be activated after the manuscript has been available in an issue.)
STATISTICS
Viewed 111 times.
AUTHORS
  • Ali Reza Molla Ebrahimlo
PDF OF ARTICLE

GRAPHICAL ABSTRACT


ABSTRACT


A facile and useful method for synthesis of 1-benzylidene semicarbazones was introduced in this work. The reaction of synthesis of the corresponding 1-benzylidene semicarbazone derivatives is carried out in the presence of acetonitrile-UHP/NH4OAc. In this method, NH4OAc was used as a source of ammonia and urea-hydrogen peroxide (UHP) as reagent. The key advantages of this process are elimination of semicarbazide, good yields and cheap reagents. All products were characterized by common techniques (infrared, 1H NMR, and melting point).

KEYWORDS
  • benzylidene semicarbazone
  • UHP
  • aromatic aldehydes
  • acetonitrile

SUPPORTING INFORMATION


Supporting Information
Download File 166-OC-2403-3177-SI.pdf (459.23 KB)