JOURNAL 2633


Organic Communications
VOLUME & ISSUE
Year: 2022 Issue: 4 October-December
PAGES
p.333 - 345
STATISTICS
Viewed 165 times.
AUTHORS
  • Doğukan Doyduk
  • Yılmaz Yildirir
PDF OF ARTICLE

GRAPHICAL ABSTRACT


ABSTRACT


Tetrazoles are frequently used in industry and medicine. However, molecules that have both tetrazole and alkenyl groups are rare. For this purpose, new 2-alkyl-5-(4-vinylphenyl)-2H-tetrazole (BF5a-i, 63-99%) derivative compounds containing both styrene and tetrazole were synthesized with a high yield under mild conditions by the Wittig reaction. Their structures were verified by spectroscopic methods (FT-IR, 1H NMR, 13C-APT NMR, HRMS, and X-Ray crystallography (for BF5a).

KEYWORDS
  • Tetrazole
  • styrene
  • X-ray crystallography
  • Wittig
  • dehydration

SUPPORTING INFORMATION


Supporting Information
Download File A3-139-OC-2211-2633-SI.pdf (7.13 MB)